亚临界萃取降低烟叶焦油及有害成分研究

田海英; 陈伟; 董艳娟; 李国政; 郝辉; 周浩; 马宇平; 聂聪; 谷令彪

doi:10.3969/j.issn.2095-476X.2015.5/6.009

CN 41-1437/TS ISSN 2096-1553

亚临界萃取降低烟叶焦油及有害成分研究

田海英 , 陈伟 , 董艳娟 , 李国政 , 郝辉 , 周浩 , 马宇平 , 聂聪 , 谷令彪

田海英, 陈伟, 董艳娟, 等. 亚临界萃取降低烟叶焦油及有害成分研究[J]. 轻工学报, 2015, 30(5-6): 43-48. doi: 10.3969/j.issn.2095-476X.2015.5/6.009

引用本文: 田海英, 陈伟, 董艳娟, 等. 亚临界萃取降低烟叶焦油及有害成分研究[J]. 轻工学报, 2015, 30(5-6): 43-48. doi: 10.3969/j.issn.2095-476X.2015.5/6.009

TIAN Hai-ying, CHEN Wei, DONG Yan-juan, et al. Study on subcritical extraction technology in reducing tar and harmful components of tobacco leaf[J]. Journal of Light Industry, 2015, 30(5-6): 43-48. doi: 10.3969/j.issn.2095-476X.2015.5/6.009

Citation: TIAN Hai-ying, CHEN Wei, DONG Yan-juan, et al. Study on subcritical extraction technology in reducing tar and harmful components of tobacco leaf[J]. Journal of Light Industry, 2015, 30(5-6): 43-48. doi: 10.3969/j.issn.2095-476X.2015.5/6.009

亚临界萃取降低烟叶焦油及有害成分研究

田海英 ¹ ,
陈伟 ¹ ,
董艳娟 ¹ ,
李国政 ¹ ,
郝辉 ¹ ,
周浩 ¹ ,
马宇平 ^{1

,} ,
聂聪 ² ,
谷令彪 ³

河南中烟工业有限责任公司技术中心, 河南郑州 450000;
中国烟草总公司郑州烟草研究院, 河南郑州 450001;
郑州大学物理工程学院, 河南郑州 450001

通讯作者: 马宇平

基金项目: 国家烟草专卖局减害重大专项项目(110201301024JH-05)
中图分类号: TS41⁺1

Study on subcritical extraction technology in reducing tar and harmful components of tobacco leaf

Technolgy Center, China Tobacco He'nan Industrial Co., Ltd., Zhengzhou 450000, China;
Zhengzhou Tobacco Research Institute of CNTC, Zhengzhou 450001, China;
College of Physical Engineering, Zhengzhou University, Zhengzhou 450001, China

Corresponding author: MA Yu-ping,

Received Date: 2015-06-05
Available Online: 2015-11-15
CLC number: TS41⁺1

摘要: 为探索降焦减害的新途径,从源头上降低卷烟中焦油及有害成分,将亚临界萃取技术引入烟叶的处理过程,对萃取条件进行优化,对用处理后烟丝制成的卷烟中主流烟气的有害成分、焦油、烟碱等释放量进行分析,同时考查处理后烟丝化学成分、加工性能及感官质量的变化情况,结果表明:用二甲醚作萃取溶剂,微波破壁处理然后萃取2次,每次30 min为最优的萃取方式;主流烟气中焦油、烟碱有明显降低,降低比例分别为33.4%和62.2%;处理后烟丝的加工性能无明显变化;7种有害成分中苯酚,HCN,NH₃,CO和B[a]P这5种成分的释放量降低明显,有害指数降低了3.87;感官评吸的柔细度、余味、刺激性均好于对照样,呈现柔、细、甜的特点.这表明,亚临界萃取技术在降低烟叶的焦油和有害成分释放量方面具有重要的应用价值.
- 亚临界萃取 /
- 烟叶 /
- 焦油 /
- 有害成分 /
- 加工性能 /
- 感官质量
Abstract: In order to investigate the new way to reduce tar and harmful components in cigarette, subcritical extraction technology was used to treat tobacco leaf.The extraction conditions were optimized.The deliveries of the harmful components, tar, nicotine in mainstream smoke of cigarettes prepared with the extracted cut tobacco were determined, the chemical components, processability and sensory quality were also evaluated.The results indicated that:microwave wall-breaking treatment, dimethyl ether extraction 2 times, each time 30 min was the optimal extraction method;the deliveries of tar and nicotine were significantly lowered than the control sample with the decreased rate at 33.4% and 62.2% respectively;the structure of extracted cut tobacco remained no obvious change; in the seven harmful components, the release amount of phenol, HCN, NH₃, CO and B[a]P were decreased.The harmful index reduced by 3.87;the sensory evalution of extracted cut tobacco was found to be superior to the controller in tender degree, aftertaste and stimulation.It was characterized by tenderness and sweetness.The study showed that subcritical extraction technology provides a potential way of reducing tar and harmful components in tobacco leaf.
- subcritical extraction /
- tobacco leaf /
- tar /
- harmful components /
- processability /
- sensory quality
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沈阳化工大学材料科学与工程学院沈阳 110142

田海英, 陈伟, 董艳娟, 等. 亚临界萃取降低烟叶焦油及有害成分研究[J]. 轻工学报, 2015, 30(5-6): 43-48. doi: 10.3969/j.issn.2095-476X.2015.5/6.009

引用本文: 田海英, 陈伟, 董艳娟, 等. 亚临界萃取降低烟叶焦油及有害成分研究[J]. 轻工学报, 2015, 30(5-6): 43-48. doi: 10.3969/j.issn.2095-476X.2015.5/6.009

亚临界萃取降低烟叶焦油及有害成分研究

通讯作者: 马宇平

河南中烟工业有限责任公司技术中心, 河南郑州 450000;
中国烟草总公司郑州烟草研究院, 河南郑州 450001;
郑州大学物理工程学院, 河南郑州 450001

收稿日期: 2015-06-05
网络出版日期: 2015-11-15

基金项目: 国家烟草专卖局减害重大专项项目(110201301024JH-05)

关键词:

摘要: 为探索降焦减害的新途径,从源头上降低卷烟中焦油及有害成分,将亚临界萃取技术引入烟叶的处理过程,对萃取条件进行优化,对用处理后烟丝制成的卷烟中主流烟气的有害成分、焦油、烟碱等释放量进行分析,同时考查处理后烟丝化学成分、加工性能及感官质量的变化情况,结果表明:用二甲醚作萃取溶剂,微波破壁处理然后萃取2次,每次30 min为最优的萃取方式;主流烟气中焦油、烟碱有明显降低,降低比例分别为33.4%和62.2%;处理后烟丝的加工性能无明显变化;7种有害成分中苯酚,HCN,NH₃,CO和B[a]P这5种成分的释放量降低明显,有害指数降低了3.87;感官评吸的柔细度、余味、刺激性均好于对照样,呈现柔、细、甜的特点.这表明,亚临界萃取技术在降低烟叶的焦油和有害成分释放量方面具有重要的应用价值.

English Abstract

Study on subcritical extraction technology in reducing tar and harmful components of tobacco leaf

Corresponding author: MA Yu-ping,

Technolgy Center, China Tobacco He'nan Industrial Co., Ltd., Zhengzhou 450000, China;
Zhengzhou Tobacco Research Institute of CNTC, Zhengzhou 450001, China;
College of Physical Engineering, Zhengzhou University, Zhengzhou 450001, China

Received Date: 2015-06-05
Available Online: 2015-11-15

Abstract: In order to investigate the new way to reduce tar and harmful components in cigarette, subcritical extraction technology was used to treat tobacco leaf.The extraction conditions were optimized.The deliveries of the harmful components, tar, nicotine in mainstream smoke of cigarettes prepared with the extracted cut tobacco were determined, the chemical components, processability and sensory quality were also evaluated.The results indicated that:microwave wall-breaking treatment, dimethyl ether extraction 2 times, each time 30 min was the optimal extraction method;the deliveries of tar and nicotine were significantly lowered than the control sample with the decreased rate at 33.4% and 62.2% respectively;the structure of extracted cut tobacco remained no obvious change; in the seven harmful components, the release amount of phenol, HCN, NH₃, CO and B[a]P were decreased.The harmful index reduced by 3.87;the sensory evalution of extracted cut tobacco was found to be superior to the controller in tender degree, aftertaste and stimulation.It was characterized by tenderness and sweetness.The study showed that subcritical extraction technology provides a potential way of reducing tar and harmful components in tobacco leaf.