WU Shuaifan, LU Chengwei, CUI Xiuming, et al. Study on the preparation process of tobacco volatiles by steam distillation and its application in electronic cigarette[J]. Journal of Light Industry, 2020, 35(1): 72-78. doi: 10.12187/2020.01.009
Citation:
WU Shuaifan, LU Chengwei, CUI Xiuming, et al. Study on the preparation process of tobacco volatiles by steam distillation and its application in electronic cigarette[J]. Journal of Light Industry, 2020, 35(1): 72-78.
doi:
10.12187/2020.01.009
Study on the preparation process of tobacco volatiles by steam distillation and its application in electronic cigarette
-
1. Shanghai Danhua Xianghua Technology Co., Ltd., Shanghai 201210, China;
-
2. Shanghai New Tobacco Products Research Institute Co., Ltd., Shanghai 200082, China
-
Received Date:
2019-07-25
-
Abstract
Tobacco volatiles were prepared by steam distillation, and the process conditions were optimized. The aroma components in tobacco volatiles were analyzed by GC-MS. The tobacco volatiles prepared under the optimal conditions were used in the preparation of electronic cigarette liquid, and its application effect was analyzed by sensory evaluation. The results showed that:The yield of tobacco volatiles prepared by distillation in water was significantly higher than that prepared by distillation over water; The best distillation conditions were 2 h infiltration time, 6 h in distillation time, and the NaCl mass fraction in the distillation system was 5%; Distilled in water, under the best distillation conditions, the aroma components in tobacco volatiles mainly include neophytadiene, solanone, damascenone, megastigmatrienone, geranylacetone, farnesylacetone, etc., but nicotine was not detected; Under the best distillation conditions and the same dilution 2000 times, the tobacco volatiles prepared by distillation in water were rich in flavor, obvious in tobacco fragrance, abundant in aroma, strong and thick in aroma, which was better than that prepared by distillation over water. Tobacco volatiles prepared under best distillation conditions by distillation in water could better meet the tobacco style and smoke state of traditional cigarettes required by electronic cigarettes.
-
-
References
-
[1]
BURSTYN L.Peering through the mist:Systematic review of what the chemistry of contaminants in electronic cigarettes tells us about health risks[J]. BMC Public Health,2014,14:18.
-
[2]
淡俊豪,齐绍武,黎娟,等.新型烟草制品用烟草香味物质提取与分离纯化技术研究进展[J].山东农业科学,2017,49(11):151.
-
[3]
窦玉青,沈轶,杨举田,等.新型烟草制品发展现状及展望[J].中国烟草科学,2016,37(5):92.
-
[4]
李翔,谢复炜,刘惠民.新型烟草制品毒理学评价研究进展[J].烟草科技,2016,47(1):88.
-
[5]
王晓杰,马越,杨国伟,等.水蒸气蒸馏法提取佛手挥发油的工艺研究[J].食品科技,2009,34(3):86.
-
[6]
丁瑞康,王承瀚,朱尊权,等.卷烟工艺学[M].北京:食品工业出版社,1958:49-50.
-
[7]
杨菁,沈晓洁,张怡春,等.烟梗的超临界CO2流体萃取工艺及萃取物在电子烟中的应用[J].烟草科技,2016,49(7):51.
-
[8]
李炎强,冼可法.同时蒸馏萃取法与水蒸气蒸馏法分离分析烟草挥发性、半挥发性中性成分的比较[J].烟草科技,2000(2):18.
-
[9]
高宏建,张献忠,钟建军,等.水蒸汽蒸馏法提取烟草精油的研究[J].食品工业科技,2011,32(10):388.
-
[10]
中华人民共和国国家质量监督检验检疫总局,中国国家标准化管理委员会.卷烟第4部分:感官技术要求:GB 5606.4-2005[S].北京:中国标准出版社,2005.
-
[11]
国家烟草专卖局.烟草及烟草制品感官评价方法:YC/T 138-1998[S].北京:中国标准出版社,1998.
-
[12]
毛多斌,贾春晓,张峻松,等.茄酮及其降解产物系列香料的合成研究进展[J].郑州轻工业学院学报,1998,13(2):57.
-
[13]
MATSUSHIMA S,ISHIGURO S,SUGAWARA S.Relationship between composition of tobacco essential oil and its aroma[J].Journal of the Agricultural Chemical Society of Japan,1980,54(12):1027.
-
[14]
李炎强,郝建辉,赵明月,等.烤烟烟梗和叶片中性香味成分的分析[J].烟草科技,2002(11):3.
-
Proportional views
-
-