JOURNAL OF LIGHT INDUSTRY

CN 41-1437/TS  ISSN 2096-1553

Volume 28 Issue 4
July 2013
Article Contents
CHEN Feng-hua, LI Shan, JIA Chun-xiao, et al. Optimization on ultrasonic-assisted extraction technology of sucrose esters from tobacco by response surface methodology[J]. Journal of Light Industry, 2013, 28(4): 15-19. doi: 10.3969/j.issn.2095-476X.2013.04.004
Citation: CHEN Feng-hua, LI Shan, JIA Chun-xiao, et al. Optimization on ultrasonic-assisted extraction technology of sucrose esters from tobacco by response surface methodology[J]. Journal of Light Industry, 2013, 28(4): 15-19. doi: 10.3969/j.issn.2095-476X.2013.04.004 shu

Optimization on ultrasonic-assisted extraction technology of sucrose esters from tobacco by response surface methodology

  • Corresponding author: JIA Chun-xiao, 
  • Received Date: 2013-06-01
    Available Online: 2013-07-15
  • The ultrasonic-assisted extraction technology of sucrose esters (SE) from tobacco was studied.The qualitative and quantitative analysis was performed by gas chromatography-mass spectrometry (GC-MS) method,and the effect of various factors including extraction solvent, temperature,time and solid liquid ratio on the total extract yield of SE was investigated by response surface methodology (RSM).The results showed that the optimal extraction conditions were as follows:the extraction solvent acetonitrile,the solid liquid ratio 1:29,the temperature 43℃ and the extraction time 16 min.Under the optimized conditions,the total extract yield of SE was 5.039 (actual) or 5.067 (theoretical),the average recovery was 99.87%,7.74% more than that obtained under the optimized conditions of single facter tests.The determination results of 10 kinds of tobacco leaf showed that the kinds and content of SE in tobacco leaves were different with different origin,variety and level.
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    1. [1]

      Severson R F,Arrendale R F,Chortyk O T,et al.Isolation and characterization of the sucrose esters of the cuticular waxes of green tobacco leaf[J].Journal of Agricultural and Food Chemistry,1985,33(5):870.

    2. [2]

      Schlotzbauer W S,Severson R F,Martin R M.The contribution of sucrose esters to tobacco smoke composition[J].Beitr Tabakfor Int,1986,13(5):229.

    3. [3]

      曾世通,李鹏,胡军.低级脂肪酸多元醇混合酯的合成及其在烟草中的加香评价[J].烟草科技,2009(3):33.

    4. [4]

      孔光辉,王伟,崔国民.烤烟烟叶腺毛及其分泌物研究进展[J].烟草农业科学,2006,2(3):235.

    5. [5]

      Severson R F,Johnson A W,Jackson D M,et al.Cuticular constituents of tobacco:Factors affecting their production and their role in insect and disease resistance and smoke quality[J].Recent Advances in Tobacco Science,1985(11):105.

    6. [6]

      Toshiake M,Koushi,Akira K.Germination and growth inhibition of surface lipids from nicotine species and identification of sucrose esters[J].Journal of Agricultural and Food Chemistry,1988,52(8):1889.

    7. [7]

      Daniel H J.Biological activity of acyl glucose esters from Datura wrightii glandular trichomes against three nativeinsect herbivores[J].Chemical Ecology,2005(31):1475.

    8. [8]

      Breda S,Marija S,Irena V.Analysis of sucrose esters-insecticides from the surface of tobacco plant leaves[J].Journal of Chromatography A,2006,1127:273.

    9. [9]

      Noel W,Einolf,Geoffrey C W.Estimation of sucrose esters in tobacco by direct chemical ionization mass spectrometry[J].Journal of Agricultural and Food Chemistry,1984(32):785.

    10. [10]

      蔡莉莉,谢复炜,谢剑平.香料烟中蔗糖酯的气相色谱/质谱分析[J].烟草科技,2009(3):40.

    11. [11]

      Li D,Xie F,Zhao M,et al.Rapid quantification of sucrose esters in oriental tobacco by liquid chromatography-ion trap mass spectrometry[J].Journal of Separation Science,2007(30):35.

    12. [12]

      Mashraf K,Taylor L T,Nazem N,et al.Isolation of tetra-acyl sucrose esters from Turkish tobacco using supercritical fluid CO2 and comparison with conventional solvent extraction[J].Journal of Agricultural and Food Chemistry,2005(53):1866.

    13. [13]

      郭青,林文强,牟定荣,等.超声波萃取技术在烟草成分分离中的应用研究综述[J].郑州轻工业学院学报:自然科学版,2011,26(5):96.

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