JOURNAL OF LIGHT INDUSTRY

CN 41-1437/TS  ISSN 2096-1553

Volume 33 Issue 5
September 2018
Article Contents
XU Aifei, ZHANG Pingquan, FAN Zhong, et al. Simultaneous determination of the content of menthol, triacetin and nicotine in mint cigarette filter by gas chromatography[J]. Journal of Light Industry, 2018, 33(5): 53-59. doi: 10.3969/j.issn.2096-1553.2018.05.007
Citation: XU Aifei, ZHANG Pingquan, FAN Zhong, et al. Simultaneous determination of the content of menthol, triacetin and nicotine in mint cigarette filter by gas chromatography[J]. Journal of Light Industry, 2018, 33(5): 53-59. doi: 10.3969/j.issn.2096-1553.2018.05.007 shu

Simultaneous determination of the content of menthol, triacetin and nicotine in mint cigarette filter by gas chromatography

  • Received Date: 2017-12-06
    Accepted Date: 2018-03-26
  • HP-Innowax capillary column was selected and the content of menthol, triacetin and nicotine in mint cigarette filter was determined by gas chromatography with anhydrous ethanol as extraction solvent. The results showed that:The linear relationship was good among menthol, triacetic acid and nicotine in the concentration range of 0.30~4.80 g·L-1, 0.30~4.80 g·L-1 and 0.01~0.16 g·L-1, respectively, the limit of quantification was 14.4 μg·branch-1,29.8 μg·branch-1 and 9.6 μg·branch-1, the spiked recoveries of the three targets ranged from 97.1% to 103.1%, and the determination result of 7 mint cigarette filter samples by this method showed that the relative standard deviations (RSD) were less than 3.0%. The content of menthol in the menthol cigarette filter was significantly higher than that of the traditional menthol cigarette filter, while the change of nicotine and triacetin content had no obvious change.
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    1. [1]

      FURRER S M,SLACK J P,Mc CLUSKEY S T,et al.New developments in the chemistry of cooling compounds[J].Chemosensory Perception,2008,1(2):119.

    2. [2]

      郑昌戈,刘煊业,喻晓蔚,等.L-薄荷醇的合成研究[J].化工进展,2011,30(10):2276.

    3. [3]

      何智慧,罗嘉,练文柳.薄荷卷烟研究进展[J].烟草科技,2006(9):38.

    4. [4]

      程阔菊,王晖,陈垦.薄荷醇的安全性研究进展[J].辽宁中医杂志,2010,37(2):377.

    5. [5]

      ECCLES R.Menthol and related cooling compounds[J].Journal of Pharmacy & Pharmacology,1994,46(8):618.

    6. [6]

      STRASSER A A,ASHARE R L,KAUFMAN M,et al.The effect of menthol on cigarette smoking behaviors,biomarkers and subjective responses[J].Cancer Epidemiol Biomarkers Prev,2013,22(3):382.

    7. [7]

      王文俊,孙凯健,陈静.薄荷醇加香位置对主流烟气中薄荷醇含量的影响[C]//中国烟草学会2014年学术年会.上海:上海市烟草学会,2014.

    8. [8]

      金闻博,戴亚,杨俊.烟草化学与烟气分析[M].南昌:江西科技出版社,1993.

    9. [9]

      周永芳,张伟杰,蒋平平.国内外烟草用增塑剂三醋酸甘油酯现状及发展趋势[J].增塑剂,2010,21(2):4.

    10. [10]

      冯剑,王军,王雷,等.滤嘴中三乙酸甘油酯含量与其物理指标的相关性研究[J].安徽农业通报,2012,16(6):126.

    11. [11]

      张卫平,陆明华,胡爱平,等.气相色谱法测定醋酸纤维滤棒中薄荷醇[J].理化检验:化学分册,2014,50(10):1299.

    12. [12]

      中国国家标准化管理委员会.醋酸纤维滤嘴中薄荷醇的测定气相色谱法:YC/T 416-2011[S].北京:中国标准出版社,2011.

    13. [13]

      中国国家标准化管理委员会.醋酸纤维滤嘴中三乙酸甘油酯的测定气相色谱法:YC/T 331-2010[S].北京:中国标准出版社,2010.

    14. [14]

      黄龙,陈一,刘辉,等.卷烟及烟气中薄荷醇的毛细气相色谱分析[J].烟草科技,2007(4):32.

    15. [15]

      宫梅,葛炯,许建铭,等.卷烟及烟气中薄荷醇含量的测定[J].烟草科技,2002(7):29.

    16. [16]

      林文强,欧亚非,王瑞玲,等.薄荷型卷烟和主流烟气中薄荷醇分析及其转移的研究[J].化学研究与应用,2010,22(9):1122.

    17. [17]

      中国国家标准化管理委员会.卷烟滤嘴中烟碱的测定气相色谱法:YC/T 154-2001[S].北京:中国标准出版社,2001.

    18. [18]

      黄华发.卷烟滤嘴中三醋酸甘油酯向主流烟气的转移研究[J].安徽农业科技,2012,40(6):3602.

    19. [19]

      中国国家标准化管理委员会.卷烟第1部分抽样:GB/T 5606.1-2004[S].北京:中国标准出版社,2004.

    20. [20]

      中国国家标准化管理委员会.卷烟用常规分析用吸烟机测定总粒相物和焦油:GB/T 19609-2004[S].北京:中国标准出版社,2004.

    21. [21]

      彭斌,孙学辉,尚平平,等.辅助材料设计参数对烤烟型卷烟烟气焦油、烟碱和CO释放量的影响[J].烟草科技,2012(2):61.

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