复凝聚法制备甜橙油纳米微胶囊的研究

李振杰; 熊亚妹; 刘远上; 张凤梅; 何沛; 许春平

doi:10.12187/2022.02.006

Volume 37 Issue 2

May 2022

Article Contents

Abstract

References

LI Zhenjie, XIONG Yamei, LIU Yuanshang, et al. Study on the preparation of sweet orange oil nanocapsules by complex coacervation[J]. Journal of Light Industry, 2022, 37(2): 44-50. doi: 10.12187/2022.02.006

Citation: LI Zhenjie, XIONG Yamei, LIU Yuanshang, et al. Study on the preparation of sweet orange oil nanocapsules by complex coacervation[J]. Journal of Light Industry, 2022, 37(2): 44-50. doi: 10.12187/2022.02.006 shu

Study on the preparation of sweet orange oil nanocapsules by complex coacervation

1. Technology Center/Key Laboratory of Tobacco Chemistry of Yunan, China Tobacco Yunnan Industrial Co., Ltd., Kunming 650231, China;
2. College of Food and Biology Engineering, Zhengzhou University of Light Industry, Zhengzhou 450001, China;
3. Technology Center, China Tobacco Hebei Industrial Co., Ltd., Shijiazhuang 050000, China

Received Date: 2020-09-23
Accepted Date: 2021-03-31

Abstract

Using chitosan as the wall material, sweet orange oil as the core material, and sodium tripolyphosphate (TPP) as the cross-linking agent, the sweet orange oil nanocapsules were prepared by the complex aggregation method. Through single factor test and orthogonal test, the process conditions were optimized, and the evaluation of particle size and distribution, surface structure, physical stability, thermal stability and embedding situation of sweet orange oil nanocapsules were analyzed. The results showed that the optimal process conditions for preparing sweet orange oil nanocapsules by complex aggregation method were chitosan mass concentration 1.8 mg/mL, tween 20 mass concentration 1.2 mg/mL, and sweet orange oil mass concentration 3.6 mg/mL; The average particle size of the sweet orange oil nano-microcapsule emulsion prepared under the optimal conditions was about 500 nm, showing a normal distribution, and the emulsion had good physical stability. The orange oil nano microcapsule had good thermal stability. Infrared spectroscopy showed that orange oil was successfully embedded in chitosan.
- complex coacervation,
- sweet orange oil,
- nanocapsule,
- chitosan,
- particle size
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