超临界CO<sub>2</sub>萃取富硒百香果籽油的工艺研究

张晗; 周利琴; 刘志国; 刘胜林; 廖丹葵

doi:10.12187/2023.03.006

June 2023

Article Contents

ZHANG Han, ZHOU Liqin, LIU Zhiguo, et al. Optimization of extraction of Selenium enriched passion fruit seed oil with supercritical CO2 extraction technology[J]. Journal of Light Industry, 2023, 38(3): 46-54. doi: 10.12187/2023.03.006

Citation: ZHANG Han, ZHOU Liqin, LIU Zhiguo, et al. Optimization of extraction of Selenium enriched passion fruit seed oil with supercritical CO2 extraction technology[J]. Journal of Light Industry, 2023, 38(3): 46-54. doi: 10.12187/2023.03.006 shu

Optimization of extraction of Selenium enriched passion fruit seed oil with supercritical CO₂ extraction technology

1. College of Chemistry and Chemical Engineering, Guangxi University, Nanning 530004, China;
2. Guangxi Pingnan Wanjiaxiang Food Co., Ltd., Guigang 537100, China

Received Date: 2022-07-27
Accepted Date: 2022-12-16

Abstract

Selenium enriched passion fruit seed oil was prepared by supercritical CO₂ extraction method with Selenium enriched passion fruit seed as raw material. Based on single factor experiment, RSM-CCD (response surface curve-central composite design) was used to explore the effects of temperature, pressure, static extraction time, dynamic extraction time and CO₂ flow rate on the extraction rate of Selenium enriched passion fruit seed oil. And the physical and chemical properties, fatty acid content and antioxidant activity of selenium-rich passionfruit seed oil extracted by supercritical CO₂extraction and Soxhlet extraction were investigated. The results showed that optimal process parameters of supercritical CO₂ extraction for oil from Selenium enriched passion seed was found to be extraction temperature of 50 ℃,extraction pressure of 34 MPa,static extraction of 109 min,dynamic extraction of 97 min, CO₂ flow rate of 1.0 L/min. Under this condition, the actual Selenium enriched passion seed oil was clear light yellow liquid, and the yield was 72.33%. The content of unsaturated fatty acids extracted by supercritical CO₂ extraction was 80.11%, which was slightly higher than that extracted by soxhlet extraction (78.71%); Acid value, peroxide value, oxidation resistance and other properties also showed that the quality of oil extracted by supercritical CO₂ extraction was better than that extracted by Soxhlet extraction.
- Selenium enriched passion fruit seed oil,
- RSM-CCD,
- supercritical CO₂ extraction method
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