辊压法全烟梗再造烟叶的制备工艺优化及结构与性能分析

许克静; 刘语煊; 张展; 吕晶晶; 梁淼; 李瑞丽; 张峻松; 陈小龙

doi:10.12187/2025.01.008

February 2025

Article Contents

XU Kejing, LIU Yuxuan, ZHANG Zhan, et al. Optimization of preparation process and analysis of structure and performance of rolled reconstituted tobacco based on whole tobacco stem[J]. Journal of Light Industry, 2025, 40(1): 64-74. doi: 10.12187/2025.01.008

Citation: XU Kejing, LIU Yuxuan, ZHANG Zhan, et al. Optimization of preparation process and analysis of structure and performance of rolled reconstituted tobacco based on whole tobacco stem[J]. Journal of Light Industry, 2025, 40(1): 64-74. doi: 10.12187/2025.01.008 shu

Optimization of preparation process and analysis of structure and performance of rolled reconstituted tobacco based on whole tobacco stem

1. Technology Center, China Tobacco Henan Industrial Co., Ltd., Zhengzhou 450003, China;
2. College of Tobacco Science and Engineering, Zhengzhou University of Light Industry, Zhengzhou 450001, China

Corresponding author: CHEN Xiaolong, cxlong119@163.com
Received Date: 2024-03-04
Accepted Date: 2024-05-11

Abstract

Tobacco stem power and tobacco leave power were used to prepare rolled reconstituted tobacco, the suitable process parameters for reconstituted tobacco based on stem were determined through orthogonal experiments. The basic physicochemical properties, microstructure, glycerol adsorption performance, thermal weight loss characteristics and released aroma components under heating conditions were compared between the reconstituted tobacco prepared from whole tobacco leaves and stem. The results showed that the optimal addition amounts of water, wood pulp fiber, and carboxymethyl cellulose sodium were 75%, 2.5%, and 5% based on tobacco stem power, respectively, from the perspective of tensile strength and sensory quality. The rolled thickness and baking temperature were selected as 0.25 mm and 90 ℃, respectively. The quantitative, tensile strength, and bulk thickness of whole stem reconstituted tobacco leaves were 265.33 g/m², 0.43 kN/m, and 0.83 cm³/g, respectively, which were superior to that of reconstituted tobacco based on whole leaves. The surface uniformity and color retention were good, the micro-pore structure was rich, and the fiber arrangement was relatively loose. The static equilibrium adsorption rate of glycerol in whole stem reconstituted tobacco was 25.0%, which was higher than that in whole leaves reconstituted tobacco. The adsorption process follows a quasi first order kinetic model and exhibited higher adsorption rate constant. Both types of whole leaves reconstituted tobacco exhibited similar four stage thermal decomposition weight loss processes. But the temperature for thermal weight loss stages Ⅱ and Ⅲ of whole stem reconstituted tobacco were more concentrated. The maximum weight loss rate and CPI of these two stages were higher than those of whole leaves reconstituted tobacco. The types and contents of aroma compounds released by whole stem reconstituted tobacco leaves in stage Ⅲ were 41, with a content of 3 410.49 μ g/g, all of which were higher than the types and contents of heat released aroma compounds in stage Ⅱ. Among them nicotine, neonicotinoid, DDMP, furfuryl alcohol and other aroma substances could be effectively released. The rolled reconstituted tobacco prepared by tobacco stem had good tensile strength and loose thickness, rich micro-pore structure, and effective release performance for aroma substances under heating conditions.The good fragrance loading capacity and low raw material cost demonstrated its potential for application in heated cigarettes.
- tobacco stem,
- rolled reconstituted tobacco,
- adsorption performance,
- thermal weight loss,
- flavor substance
References
1. [1]
  张金磊,秦云华,杨柳,等.造纸法再造烟叶品质提升技术研究进展[J].安徽农学通报,2023,29(5):116-121.
2. [2]
  BOUÉ S,SCHLAGE W K,PAGE D,et al.Toxicological assessment of tobacco heating system 2.2:Findings from an independent peer review[J].Regulatory Toxicology and Pharmacology,2019,104:115-127.
3. [3]
  赵玉宇,崔成哲,朱良华,等.加热不燃烧烟草制品的减害性能分析[J].科技创新与应用,2020,10(22):66-67.
4. [4]
  SIMONAVICIUS E,MCNEILL A,SHAHAB L,et al.Heat-not-burn tobacco products:A systematic literature review[J].Tobacco Control,2019,28(5):582-594.
5. [5]
  卢乐华,高洁,费菲,等.不同工艺电加热卷烟再造烟叶主要成分的释放性能[J].烟草科技,2023,56(3):30-40
  ,77.
6. [6]
  李奕蓉,汤丹瑜,刘春波,等.三种新型工艺加热卷烟再造烟叶的对比[J].烟草科技,2023,56(6):59-68.
7. [7]
  杨菁,赵文涛,艾明欢,等.不同类型的加热卷烟原料性能比较[J].中国烟草学报,2020,26(3):1-8.
8. [8]
  司晓喜,唐石云,朱瑞芝,等.不同原料稠浆法再造烟叶加热卷烟的气溶胶释放特性[J].中国烟草学报,2021,27(6):1-9.
9. [9]
  赵璐,王丙武,宋中邦,等.基于感官评价的加热不燃烧卷烟原料品种(系)筛选[J].烟草科技,2020,53(1):21-28.
10. [10]
  苏丹丹,王小升,张文军,等.不同梗叶比例对造纸法再造烟叶片基的影响[J].纸和造纸,2019,38(1):28-31.
11. [11]
  董高峰,田永峰,唐石云,等.梗叶配比对加热卷烟专用稠浆法再造烟叶品质的影响[J].中国烟草学报,2021,27(1):31-36.
12. [12]
  郭春生,王轶群,陈晨,等.甘油对不同部位烤烟香味成分释放行为的影响[J].中国烟草科学,2023,44(2):88-96.
13. [13]
  中华人民共和国国家质量监督检验检疫总局.纸和纸板抗张强度的测定恒速拉伸法:GB/T12914—2018[S].北京:中国标准出版社,2018.
14. [14]
  中华人民共和国国家质量监督检验检疫总局.纸和纸板定量的测定:GB/T 451.2—2002[S].北京:中国标准出版社,2002.
15. [15]
  中华人民共和国国家质量监督检验检疫总局.纸和纸板厚度的测定:GB/T 451.3—2002[S].北京:中国标准出版社,2002.
16. [16]
  国家烟草专卖局.烟草及烟草制品水溶性糖的测定连续流动法:YC/T 159—2002[S].北京:中国标准出版社,2002.
17. [17]
  国家烟草专卖局.烟草及烟草制品总氮的测定连续流动法:YC/T 161—2002[S].北京:中国标准出版社,2002.
18. [18]
  国家烟草专卖局.烟草及烟草制品钾的测定连续流动法:YC/T 217—2007[S].北京:中国标准出版社,2007.
19. [19]
  国家烟草专卖局.烟草及烟草制品氯的测定连续流动法:YC/T 162—2011[S].北京:中国标准出版社,2011.
20. [20]
  国家烟草专卖局.烟草及烟草制品烟碱的测定气相色谱法:YC/T 246—2008[S].北京:中国标准出版社,2008.
21. [21]
  刘天择,杨菁,汪旭,等.不同部位烤烟化学成分及热解产物与加热卷烟感官质量的关系[J].中国烟草科学,2023,44(1):77-84.
22. [22]
  朱宏阳,姚俊,冯珊,等.1株产细菌纤维素芽胞杆菌的分离及鉴定[J].生物加工过程,2014,12(5):80-84.
23. [23]
  PAREEK N,GILLGREN T,JÖNSSON L J.Adsorption of proteins involved in hydrolysis of lignocellulose on lignins and hemicelluloses[J].Bioresource Technology,2013,148:70-77.
24. [24]
  高峄涵,李祥林,冯智渊,等.3种电加热卷烟专用再造烟叶的甘油饱和吸附特性[J].烟草科技,2022,55(5):41-49.
25. [25]
  艾明欢,杨菁,沈轶,等.TG-FTIR联用研究HnB烟草基质在400 ℃以下的热解特性和气相产物[J].中国烟草学报,2020,26(1):8-14.
26. [26]
  霍现宽,刘珊,崔凯,等.加热状态下烟草烟气香味成分释放特征[J].烟草科技,2017,50(8):37-45.
27. [27]
  唐培培,曾世通,刘珊,等.甘油对烟叶热性能及加热状态下烟气释放的影响[J].烟草科技,2015,48(3):61-65.
28. [28]
  王玉华,褚建忠,徐丙升,等.烤烟自然醇化过程美拉德反应产物变化及与感官质量的关系[J].中国烟草科学,2015,36(4):85-90.
29. [29]
  白冰,何静,杨静,等.美拉德反应中间体二氢-3,5-二羟基-6-甲基-4(H)吡喃-4-酮的研究进展[J].食品与发酵工业,2024,50(5):326-333.
Proportional views

Get Citation

PDF

XML

Article Metrics

Article views(81) PDF downloads(4) Cited by()

Ralated

通讯作者: 陈斌, bchen63@163.com

1.
沈阳化工大学材料科学与工程学院沈阳 110142

Optimization of preparation process and analysis of structure and performance of rolled reconstituted tobacco based on whole tobacco stem

Abstract

References

Proportional views

Article Metrics

Ralated

Proportional views

通讯作者: 陈斌, bchen63@163.com