JOURNAL OF LIGHT INDUSTRY

CN 41-1437/TS  ISSN 2096-1553

Volume 40 Issue 5
October 2025
Article Contents
SHI Qingzhao, FAN Wu, REN Ruibing, et al. Preparation of refined products of tobacco extracts based on membrane separation and column chromatography techniques[J]. Journal of Light Industry, 2025, 40(5): 101-109. doi: 10.12187/2025.05.012
Citation: SHI Qingzhao, FAN Wu, REN Ruibing, et al. Preparation of refined products of tobacco extracts based on membrane separation and column chromatography techniques[J]. Journal of Light Industry, 2025, 40(5): 101-109. doi: 10.12187/2025.05.012 shu

Preparation of refined products of tobacco extracts based on membrane separation and column chromatography techniques

  • To make full use of discarded tobacco leaves and develop a diverse range of refined products, tobacco extract was prepared from discarded tobacco leaves by heating extraction with an ethanol aqueous solution. The tobacco extract was then refined using membrane separation and two-dimensional column chromatography techniques. We used sensory evaluation to screen out characteristic flavor groups with prominent style features and explored the recombination process among these characteristic flavor groups. Py-GC-MS was used to analyze the recombinant products. The results showed that the yield of tobacco extract obtained by heating extraction with an ethanol aqueous solution was the highest, and the overall sensory effect was good. A total of 16 groups were obtained through refining, among which the sensory effects of the 5 nm retentate from membrane separation and the A1, C1, and E2 fractions from column chromatography separation showed distinct characteristics, serving as the characteristic flavor groups of tobacco extracts. Among the recombinant samples, samples 1# and 2# could enhance the characteristics of tobacco aroma, baking aroma, light aroma, and sweet aroma of cigarettes, and have a good overall sensory effect. The pyrolysis products of recombinant samples 1# and 2#were mainly composed of heterocyclic and aromatic compounds, including sweet, light, nutty, and other aroma types.
  • 加载中
    1. [1]

      王中山,赵静宜,杨正军,等.制丝加工过程烟叶损耗监控模型的建立及应用[J].农产品加工,2022(6):76-78,87.

    2. [2]

      谷彦岭,陈治岍,张长安,等.废弃烟草同时提取烟碱及制备浸膏的研究[J].农产品加工,2022(5):20-23.

    3. [3]

      陈芊如,孟娜,马斯琦,等.烟草废弃物资源综合利用研究进展[J].江西农业学报,2024,36(1):146-153.

    4. [4]

      朱垧榕,陈飞龙,赵伦旭,等.废弃烟叶分段式提取制备特色烟用香料[J].香料香精化妆品,2024(2):94-98.

    5. [5]

      LI Y C,ZHOU J T,XU W L,et al.Key aroma components in Lu’an Guapian green tea with different aroma types from five tea tree varieties decoded by sensomics[J].Food Bioscience,2024,61:104551.

    6. [6]

      WANG L H,QIAO K N,HUANG Y,et al.Optimization of beef broth processing technology and isolation and identification of flavor peptides by consecutive chromatography and LC-QTOF-MS/MS[J].Food Science & Nutrition,2020,8(8):4463-4471.

    7. [7]

      HUANG Y,DUAN W,WANG L H,et al.Orthogonal optimization of beef stir-fried process followed by isolation and identification of the umami peptides by consecutive chromatography and LC-Q-TOF/MS[J].International Journal of Food Properties,2019,22(1):1773-1785.

    8. [8]

      LU Q,QIU C H,ZHU J S,et al.Elucidation of key fatty aroma compound contributing to the hepatopancreas of Eriocheir sinensis using sensomics approach by GC-IMS and GC-MS-O[J].Food Chemistry,2024,455:139904.

    9. [9]

      JIANG L,SHEN S W,ZUO A T,et al.Unveiling the aromatic differences of low-salt Chinese horse bean-chili-paste using metabolomics and sensomics approaches[J].Food Chemistry,2024,445:138746.

    10. [10]

      吴彦,俞金伟,黄东业,等.膜分离技术精制罗汉果香味成分及应用[J].烟草科技,2019,52(7):51-60.

    11. [11]

      曹珂,孙志涛,杨春强,等.白肋烟提取物的分离及在卷烟中的应用[J].生物化工,2022,8(1):87-91.

    12. [12]

      郑建宇,刘晶,周桂园,等.超滤膜组合技术对烟草提取物化学成分的影响[J].烟草科技,2019,52(12):70-78.

    13. [13]

      张启东,刘俊辉,柴国璧,等.卷烟主流烟气粒相物酸味成分感官导向分析[J].烟草科技,2019,52 (11):30-40.

    14. [14]

      朱浩,柴国璧,迟广俊,等.卷烟主流烟气烟熏香成分的感官导向分析[J].烟草科技,2017,50(1):41-49.

    15. [15]

      王丁众,张启东,刘俊辉,等.烟气苦味成分的感官导向鉴定和液相色谱-高分辨质谱分析[J].质谱学报,2016,37(5):414-421.

    16. [16]

Article Metrics

Article views(322) PDF downloads(4) Cited by()

Ralated
    通讯作者: 陈斌, bchen63@163.com
    • 1. 

      沈阳化工大学材料科学与工程学院 沈阳 110142

    1. 本站搜索
    2. 百度学术搜索
    3. 万方数据库搜索
    4. CNKI搜索

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return