响应面法优化直链淀粉-正葵醇复合物制备条件的研究

潘慧慧; 闫溢哲; 林海; 史苗苗; 杨留枝; 刘延奇

doi:10.3969/j.issn.2096-1553.2016.6.003

CN 41-1437/TS ISSN 2096-1553

响应面法优化直链淀粉-正葵醇复合物制备条件的研究

潘慧慧 , 闫溢哲 , 林海 , 史苗苗 , 杨留枝 , 刘延奇

潘慧慧, 闫溢哲, 林海, 等. 响应面法优化直链淀粉-正葵醇复合物制备条件的研究[J]. 轻工学报, 2016, 31(6): 16-23. doi: 10.3969/j.issn.2096-1553.2016.6.003

引用本文: 潘慧慧, 闫溢哲, 林海, 等. 响应面法优化直链淀粉-正葵醇复合物制备条件的研究[J]. 轻工学报, 2016, 31(6): 16-23. doi: 10.3969/j.issn.2096-1553.2016.6.003

PAN Hui-hui, YAN Yi-zhe, LIN Hai, et al. Research on optimization of amylose-n-decanol complex preparation by response surface methodology[J]. Journal of Light Industry, 2016, 31(6): 16-23. doi: 10.3969/j.issn.2096-1553.2016.6.003

Citation: PAN Hui-hui, YAN Yi-zhe, LIN Hai, et al. Research on optimization of amylose-n-decanol complex preparation by response surface methodology[J]. Journal of Light Industry, 2016, 31(6): 16-23. doi: 10.3969/j.issn.2096-1553.2016.6.003

响应面法优化直链淀粉-正葵醇复合物制备条件的研究

郑州轻工业学院食品与生物工程学院, 河南郑州 450001;
鹤壁职业技术学院, 河南鹤壁 458030

通讯作者: 刘延奇

基金项目: 国家自然科学基金项目（21376228）；河南省科技基础研究项目（162300410141）
中图分类号: TS231

Research on optimization of amylose-n-decanol complex preparation by response surface methodology

College of Food and Biolengineering, Zhengzhou University of Light Industry, Zhengzhou 450001, China;
Hebi Polytechnic College, Hebi 458030, China

Corresponding author: LIU Yan-qi,

Received Date: 2016-05-11
Available Online: 2016-12-15
CLC number: TS231

摘要: 以马铃薯B型微晶直链淀粉和正葵醇为原料，采用溶剂法合成直链淀粉-正葵醇复合物，研究了乙醇浓度、直链淀粉与正葵醇的质量体积比、结晶温度等因素对该复合物结晶度的影响，建立了二次多项式回归模型.在单因素试验基础上，采用Box-Behnken响应面法试验优化了复合物的制备工艺条件.结果表明，直链淀粉-正葵醇复合物的最佳复合工艺条件为乙醇浓度7.80%，直链淀粉与正葵醇质量体积比（g：L）10：2.6，结晶温度55℃.在此条件下，预测产品结晶度将达到63.25%，验证试验所得产品平均结晶度为62.97%，说明该模型可靠性良好.
- 直链淀粉 /
- 正葵醇 /
- V-型复合物 /
- 响应面法
Abstract: Amylose-n-decanol complex was prepared by solvent method with B-type crystallite potato to amylose and n-decanol as raw material. The effects on complex synthesis process by the three factors of ethanol concentration, the ratio of quality and volume of amylose to n-decanol, crystallization temperature were discussed.The quadratic polynominal model was established.On the basis of single factor test, the optimum complex synthesis process was obtained through Box-Behnken experimental design. The results showed that the optimum complex synthesis process of amylose and n-decanol was additive amount of ethanol concentration 7.80%,the ratio of quality and volume of amylose to n-decanol (g:L) 10:2.6, crystallization temperature 55℃.The degree of crystallization of amylose-n-decanol complex forecasted will be to 63.25%.Under this condition, the products crystallinity on average achieved from verification test is 62.97%,and the model reliabitily is good.
- amylose /
- n-decanol /
- V-type complex /
- response surface methodology
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沈阳化工大学材料科学与工程学院沈阳 110142

潘慧慧, 闫溢哲, 林海, 等. 响应面法优化直链淀粉-正葵醇复合物制备条件的研究[J]. 轻工学报, 2016, 31(6): 16-23. doi: 10.3969/j.issn.2096-1553.2016.6.003

响应面法优化直链淀粉-正葵醇复合物制备条件的研究

通讯作者: 刘延奇

郑州轻工业学院食品与生物工程学院, 河南郑州 450001;
鹤壁职业技术学院, 河南鹤壁 458030

收稿日期: 2016-05-11
网络出版日期: 2016-12-15

基金项目: 国家自然科学基金项目（21376228）；河南省科技基础研究项目（162300410141）

关键词:

摘要: 以马铃薯B型微晶直链淀粉和正葵醇为原料，采用溶剂法合成直链淀粉-正葵醇复合物，研究了乙醇浓度、直链淀粉与正葵醇的质量体积比、结晶温度等因素对该复合物结晶度的影响，建立了二次多项式回归模型.在单因素试验基础上，采用Box-Behnken响应面法试验优化了复合物的制备工艺条件.结果表明，直链淀粉-正葵醇复合物的最佳复合工艺条件为乙醇浓度7.80%，直链淀粉与正葵醇质量体积比（g：L）10：2.6，结晶温度55℃.在此条件下，预测产品结晶度将达到63.25%，验证试验所得产品平均结晶度为62.97%，说明该模型可靠性良好.

English Abstract

Research on optimization of amylose-n-decanol complex preparation by response surface methodology

Corresponding author: LIU Yan-qi,

College of Food and Biolengineering, Zhengzhou University of Light Industry, Zhengzhou 450001, China;
Hebi Polytechnic College, Hebi 458030, China

Received Date: 2016-05-11
Available Online: 2016-12-15

Abstract: Amylose-n-decanol complex was prepared by solvent method with B-type crystallite potato to amylose and n-decanol as raw material. The effects on complex synthesis process by the three factors of ethanol concentration, the ratio of quality and volume of amylose to n-decanol, crystallization temperature were discussed.The quadratic polynominal model was established.On the basis of single factor test, the optimum complex synthesis process was obtained through Box-Behnken experimental design. The results showed that the optimum complex synthesis process of amylose and n-decanol was additive amount of ethanol concentration 7.80%,the ratio of quality and volume of amylose to n-decanol (g:L) 10:2.6, crystallization temperature 55℃.The degree of crystallization of amylose-n-decanol complex forecasted will be to 63.25%.Under this condition, the products crystallinity on average achieved from verification test is 62.97%,and the model reliabitily is good.

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