薄荷颗粒香料的干燥工艺及滤棒加香应用研究
Drying process of peppermint granular spices and its application in flavoring filter rod
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摘要: 为减少薄荷颗粒香料在干燥过程中特征成分的损失,建立了不同干燥条件下(烘箱干燥、微波真空干燥、微波干燥)香料的干燥动力学模型,结合水分分布的变化规律及特征成分的挥发情况优选适宜的香料干燥条件,并考查了薄荷颗粒香料的卷烟滤棒加香效果。结果表明:薄荷颗粒香料在烘箱干燥、微波真空干燥、微波干燥下的干燥时间分别约为60~120 min、20 min、4 min,3种干燥方式的最适动力学模型为Page模型;随着干燥的进行,半结合水转变为结合水和自由水,同时自由水在不断地挥发;薄荷颗粒香料特征成分均随着水分的挥发而降低,干燥温度越高,特征成分散失越明显,特征成分保留量与结合水相对峰面积呈极显著正相关;结合干燥时间及留香效果,确定微波干燥为最佳干燥工艺;薄荷颗粒香料加香后的卷烟烟气中酸类物质和酚类物质含量略有降低,酮类物质含量略有增加,新增3种薄荷特有的特征成分薄荷醇、L-薄荷酮、胡薄荷酮,在保留卷烟原有风格特征的前提下,可为卷烟带来清凉感,降低刺激性,提高卷烟的吸食品质。Abstract: In order to reduce the loss of diagnostic components of peppermint granule spices during the drying process, the moisture drying kinetics of peppermint granules under different drying conditions (oven drying, microwave vacuum drying and microwave drying) were studied. By investigating changes in moisture distribution and the volatilization of characteristic components, the authors determined the optional drying conditions for the spices. The flavoring effect of cigarette filter rod of peppermint granular spices was investigated. The results showed that the drying time of peppermint granular spices under oven drying, microwave vacuum drying and microwave drying was about 60~120 min, 20 min and 4 min, respectively. The optimal drying kinetic model of the three drying methods is the Page model. The results of LF-NMR analysis showed that with the progress of drying, the semi-bound water was transformed into bound water and free water. At the same time, free water is constantly evaporating and being removed. The concentrations of diagnostic components in peppermint granular spices decreased with the decrease of moisture content, and the higher the drying temperature, the more obvious the diagnostic components loss. The effect of microwave drying is better than microwave vacuum drying, and the drying time is greatly shortened. The residue of diagnostic components positively correlated with the peak area of the bound water. The acids and phenolic substances in the cigarette smoke after the spice of peppermint granular spices were slightly reduced, the ketones were slightly increased, and three kinds of diagnostic components unique to peppermint, menthol, L-menthol and menthone were added, which could bring a cooling feeling to the cigarette, reduce the sense of irritation and improve the smoking quality of cigarettes, while retaining the original style of cigarettes.
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Key words:
- granular spice /
- peppermint /
- drying process /
- filter rod flavoring /
- microwave drying
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