基于分子感官科学的烟用香精关键香气活性成分分析

杨鹏飞; 张增辉; 何春雨; 杨靖; 贾春晓; 毛多斌

doi:10.12187/2021.02.005

CN 41-1437/TS ISSN 2096-1553

杨鹏飞 , 张增辉 , 何春雨 , 杨靖 , 贾春晓 , 毛多斌

杨鹏飞, 张增辉, 何春雨, 等. 基于分子感官科学的烟用香精关键香气活性成分分析[J]. 轻工学报, 2021, 36(2): 34-42. doi: 10.12187/2021.02.005

引用本文: 杨鹏飞, 张增辉, 何春雨, 等. 基于分子感官科学的烟用香精关键香气活性成分分析[J]. 轻工学报, 2021, 36(2): 34-42. doi: 10.12187/2021.02.005

YANG Pengfei, ZHANG Zenghui, HE Chunyu, et al. Analysis of key aroma-active constituents in tobacco flavors based on molecular sensory science[J]. Journal of Light Industry, 2021, 36(2): 34-42. doi: 10.12187/2021.02.005

Citation: YANG Pengfei, ZHANG Zenghui, HE Chunyu, et al. Analysis of key aroma-active constituents in tobacco flavors based on molecular sensory science[J]. Journal of Light Industry, 2021, 36(2): 34-42. doi: 10.12187/2021.02.005

基于分子感官科学的烟用香精关键香气活性成分分析

1. 郑州轻工业大学食品与生物工程学院, 河南郑州 450001;
2. 郑州轻工业大学材料与化学工程学院, 河南郑州 450001

作者简介: 杨鹏飞(1981-),男,河南省洛阳市人,郑州轻工业大学讲师,博士,主要研究方向为烟草香精香料.;

基金项目: 国家自然科学基金青年基金资助项目（81903507）；郑州轻工业大学博士科研启动基金项目（0123-13501050063）
中图分类号: TS41⁺1

Analysis of key aroma-active constituents in tobacco flavors based on molecular sensory science

1. College of Food and Bioengineering, Zhengzhou University of Light Industry, Zhengzhou 450001, China;
2. College of Material and Chemical Engineering, Zhengzhou University of Light Industry, Zhengzhou 450001, China
Received Date: 2020-09-27

CLC number: TS41⁺1

摘要: 采用同时蒸馏萃取结合气相色谱-质谱联用技术分析烟用香精中的挥发性成分，利用气相色谱-质谱-嗅觉检测器联用技术结合香气提取稀释分析确定其香气活性成分，同时对香气活性成分进行定量分析并计算其香气活性值，通过香气重组实验与缺失实验确定烟用香精的关键性香气活性成分.结果表明：在烟用香精中共鉴定出54种挥发性成分，其中有22种香气活性成分；结合香气稀释因子和香气活性值确定了17种重要香气活性成分；最终确定烟用香精中的关键香气活性成分为β-大马酮、芳樟醇、乙基麦芽酚、乙酸芳樟酯、乙酸橙花酯、月桂烯、橙花醇、乙酸香叶酯、D-柠檬烯、苯甲醇.
- 烟用香精 /
- 气相色谱-质谱-嗅觉检测器联用技术 /
- 香气活性成分 /
- 香气活性值
Abstract: The volatile chemical components of tobacco flavor were prepared by simultaneous distillation extraction and analyzed using gas chromatography-mass spectrometry.The aroma-active violates were determined by means of gas chromatography-mass spectrometry-olfactometry combined with aroma extraction dilution analysis,and the important odorants were further screened out according to quantitative study and odor activity values.Aroma recombination and omission experiments identified the key odorants of the tobacco flavor.The results exhibited that simultaneous distillation extraction of tobacco flavor included 54 kinds of volatile compounds,including 22 aroma-active compounds,and 17 odorants were screened out as the predominant odorants according to flavor dilution factors and odor activity values.β-damascarone,linalool,ethyl maltol,linalyl acetate,neryl acetate,myrcene,nerol,geranyl acetate,D-limonene,and benzyl alcohol were confirmed as the key odorants of tobacco flavor.
- tobacco flavor /
- GC-MS-O /
- aroma-active constituent /
- odor activity value
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1.
沈阳化工大学材料科学与工程学院沈阳 110142

杨鹏飞, 张增辉, 何春雨, 等. 基于分子感官科学的烟用香精关键香气活性成分分析[J]. 轻工学报, 2021, 36(2): 34-42. doi: 10.12187/2021.02.005

引用本文: 杨鹏飞, 张增辉, 何春雨, 等. 基于分子感官科学的烟用香精关键香气活性成分分析[J]. 轻工学报, 2021, 36(2): 34-42. doi: 10.12187/2021.02.005

基于分子感官科学的烟用香精关键香气活性成分分析

作者简介:杨鹏飞(1981-),男,河南省洛阳市人,郑州轻工业大学讲师,博士,主要研究方向为烟草香精香料.

1. 郑州轻工业大学食品与生物工程学院, 河南郑州 450001;
2. 郑州轻工业大学材料与化学工程学院, 河南郑州 450001

收稿日期: 2020-09-27

基金项目: 国家自然科学基金青年基金资助项目（81903507）；郑州轻工业大学博士科研启动基金项目（0123-13501050063）

关键词:

摘要: 采用同时蒸馏萃取结合气相色谱-质谱联用技术分析烟用香精中的挥发性成分，利用气相色谱-质谱-嗅觉检测器联用技术结合香气提取稀释分析确定其香气活性成分，同时对香气活性成分进行定量分析并计算其香气活性值，通过香气重组实验与缺失实验确定烟用香精的关键性香气活性成分.结果表明：在烟用香精中共鉴定出54种挥发性成分，其中有22种香气活性成分；结合香气稀释因子和香气活性值确定了17种重要香气活性成分；最终确定烟用香精中的关键香气活性成分为β-大马酮、芳樟醇、乙基麦芽酚、乙酸芳樟酯、乙酸橙花酯、月桂烯、橙花醇、乙酸香叶酯、D-柠檬烯、苯甲醇.

English Abstract

Analysis of key aroma-active constituents in tobacco flavors based on molecular sensory science

1. College of Food and Bioengineering, Zhengzhou University of Light Industry, Zhengzhou 450001, China;
2. College of Material and Chemical Engineering, Zhengzhou University of Light Industry, Zhengzhou 450001, China

Received Date: 2020-09-27

Abstract: The volatile chemical components of tobacco flavor were prepared by simultaneous distillation extraction and analyzed using gas chromatography-mass spectrometry.The aroma-active violates were determined by means of gas chromatography-mass spectrometry-olfactometry combined with aroma extraction dilution analysis,and the important odorants were further screened out according to quantitative study and odor activity values.Aroma recombination and omission experiments identified the key odorants of the tobacco flavor.The results exhibited that simultaneous distillation extraction of tobacco flavor included 54 kinds of volatile compounds,including 22 aroma-active compounds,and 17 odorants were screened out as the predominant odorants according to flavor dilution factors and odor activity values.β-damascarone,linalool,ethyl maltol,linalyl acetate,neryl acetate,myrcene,nerol,geranyl acetate,D-limonene,and benzyl alcohol were confirmed as the key odorants of tobacco flavor.