辊压法薄片料液微胶囊的制备及其在电子烟烟油中的应用

许春平; 梁佳欣; 张弛; 黄家乐; 贾学伟; 李天笑; 郝辉

doi:10.12187/2023.04.013

August 2023

Article Contents

XU Chunping, LIANG Jiaxin, ZHANG Chi, et al. Preparation of casing solution microcapsules of rolled tobacco sheet and its application in electronic cigarette oil[J]. Journal of Light Industry, 2023, 38(4): 98-104. doi: 10.12187/2023.04.013

Citation: XU Chunping, LIANG Jiaxin, ZHANG Chi, et al. Preparation of casing solution microcapsules of rolled tobacco sheet and its application in electronic cigarette oil[J]. Journal of Light Industry, 2023, 38(4): 98-104. doi: 10.12187/2023.04.013 shu

Preparation of casing solution microcapsules of rolled tobacco sheet and its application in electronic cigarette oil

1. College of Tobacco Science and Engineering, Zhengzhou University of Light Industry, Zhengzhou 450001, China;
2. Technical Center, China Tobacco Henan Industrial Co., Ltd., Zhengzhou 450016, China

Received Date: 2022-06-29
Accepted Date: 2022-10-02

Abstract

To improve the release performance of aroma substances and the sensory evaluation quality of electronic cigarette, the application effect of casing solution microcapsule in electronic cigarette liquid was investigated. Firstly, the casing solution of rolled tobacco sheet was microencapsulated by the complex coacervation method, then the physical and chemical properties of the microcapsules were characterized, and the aroma components released were analyzed. Finally, the microcapsules were added to the electronic cigarette liquid for sensory evaluation. The results showed that the appearance was approximately spherical or ellipsoidal, and the structure was dense. The average particle size was about 220 nm, with uniform size and concentrated distribution, the embedding rate was 45.68%, and the moisture content was 7.39% after 7 days under the room temperature, which was easy to transport and store. After microencapsulation of the casing solution, the thermal stability was improved, and the temperature of the maximum mass loss rate of the microcapsules was about 170℃ higher than that of the casing solution. A total of 20 volatile aroma compounds were detected in microcapsules, with a total content of 1158.11 μg/g. The main aromatic substances were esters, accounting for 78.71% of the total content, which had an important impact on the flavor and taste of tobacco products. The electronic cigarette with microencapsulated tobacco oil had a better evaluation effect, reducing irritation and increasing amount of aroma, improving the puff-by-puff consistency of aroma to a certain extent.
- complex coacervation method,
- microcapsules,
- casing solution of rolled tobacco sheet,
- electronic cigarette,
- cigarette oil
References
1. [1]
  刘鸿, 张怡春, 陆怡峰, 等.电子烟气溶胶成分释放的主要影响因素[J].烟草科技, 2020, 53(10):39-45.
2. [2]
  DOMINIKA C, AIDA K, BARBARA K, et al.Influence of electronic cigarettes on selected physicochemical properties of saliva[J].International Journal of Environmental Research and Public Health, 2022, 19(6):3314.
3. [3]
  李翔, 严大为, 赵阁, 等.新型烟草制品风险评估框架要求研究进展及建议[J].烟草科技, 2021, 54(5):100-112.
4. [4]
  JI Z, TANG Y, WANG C Y, et al.Preparation of submicron capsules containing fragrance and their application as emulsifier[J].Polymer Bulletin, 2020, 78(4):1821-1833.
5. [5]
  张兰.丁香精油壳聚糖纳米微胶囊的研究及在蓝莓保鲜中的应用[D].西安:陕西科技大学, 2021.
6. [6]
  钟秋夏, 郑海英, 朱燕丽, 等.百里香酚微胶囊的制备及其对草莓的保鲜效果[J].食品科学, 2023, 44(11)167-176.
7. [7]
  赵晓晴.尼古丁系列化合物合成、结构表征及其在电子烟中的缓释效果研究[D]. 昆明:云南大学, 2019.
8. [8]
  彭莹芸.葡萄柚精油微胶囊的制备及稳定性研究[D].长沙:湖南大学, 2019.
9. [9]
  巩效伟, 张霞, 陆欣宇, 等.β-环糊精微胶囊的制备及其在电子烟烟液中的应用[J].烟草科技, 2019, 52(4):33-43.
10. [10]
  徐子淇.壳聚糖:阿拉伯胶复凝聚制备芳樟醇微胶囊的研究[D].上海:上海应用技术大学, 2018.
11. [11]
  李振杰, 熊亚妹, 刘远上, 等.复凝聚法制备甜橙油纳米微胶囊的研究[J].轻工学报, 2022, 37(2):44-50.
12. [12]
  蒋天艳, 刘婉嫕, 王聪, 等.壳聚糖/明胶/纤维素纳米晶体复合壁材制备香精微胶囊[J].中国造纸, 2021, 40(6):34-39.
13. [13]
  李佳釔, 方佳兴, 李亚隆, 等.酶解大豆蛋白复合凝聚微胶囊的制备及其性质表征[J].食品与发酵工业, 2021, 47(10):1-7.
14. [14]
  刘品, 刘寅, 张艳, 等.干燥介质相对湿度对红枣热风干燥特性的影响[J].食品与发酵工业, 2019, 45(11):185-190.
15. [15]
  张霞, 李寿波, 管莹, 等.凝胶态烟油的制备及在电子烟中的应用[J].中国烟草学报, 2021, 27(5):28-36.
16. [16]
  云南中烟工业有限责任公司.一种用于电子烟的香精香料的评价方法:202210171391.8[P].2022-02-24.
17. [17]
  黄芳丽, 唐婷范, 朱家庆, 等.蒜头果油微胶囊制备工艺优化及性质分析[J].中国油脂, 2021, 46(12):88-94.
18. [18]
  郭阳, 包怡红, 赵楠.复凝聚法制备松籽油微胶囊工艺优化及其氧化稳定性分析[J].食品科学, 2017, 38(18):229-236.
19. [19]
  赵梦月, 段续, 任广跃, 等.山茱萸黄酮微胶囊制备工艺及性质研究[J].食品与发酵工业, 2023, 49(7):181-189.
20. [20]
  TANG L Q, LIU H C, HUANG G D, et al.The structural characterization, physicochemical properties, and stability of gardenia yellow pigment microcapsules[J].LWT, 2022, 162:113507.
21. [21]
  CHAIB S, BENALI N, ARHAB R, et al.Preparation of thymus vulgaris essential oil microcapsules by complex coacervation and direct emulsion:Synthesis, characterization and controlled release properties[J].Arabian Journal for Science and Engineering, 2021, 46:5429-5446.
22. [22]
  刘云飞, 郭琪, 姬小明, 等.巨豆三烯酮-β-环糊精包合物的制备及其卷烟加香应用[J].陕西科技大学学报, 2022, 40(4):94-99.
23. [23]
  于少藤.烟叶有益微生物的筛选及其对烟叶品质改良的研究[D].南京:南京农业大学, 2020.
Proportional views

Get Citation

PDF

XML

Article Metrics

Article views(3468) PDF downloads(15) Cited by()

Ralated

通讯作者: 陈斌, bchen63@163.com

1.
沈阳化工大学材料科学与工程学院沈阳 110142

Preparation of casing solution microcapsules of rolled tobacco sheet and its application in electronic cigarette oil

Abstract

References

Proportional views

Article Metrics

Ralated

Proportional views

通讯作者: 陈斌, bchen63@163.com