两种雪茄烟分段烟气香气成分及香气特征差异分析
Differential analysis of aroma compounds and aroma profiles of segmented smoke of two types of cigar
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摘要: 为探究雪茄烟前、中、后3段烟气的差异性,采用气相色谱-质谱联用技术(GC-MS)对长城2号和蒙特4号两种雪茄烟分段烟气香气成分进行检测,结合感官评价和气味贡献权重对雪茄烟香气特征进行研究,并基于偏最小二乘判别分析(PLS-DA)法筛选雪茄烟中关键差异香气成分。结果表明:抽吸过程中烟支变短、截留效果减弱,雪茄烟烟气中香气成分的数量和释放量整体呈增加趋势;在雪茄烟气味贡献权重中,随着抽吸的进行,长城2号的豆香和木香减弱、咖啡香增强,蒙特4号的豆香减弱、辛香增强,这些气味的权重变化与感官评价结果具有一致性;长城2号中引起香气特征变化的有γ-己内酯、糠酸、苯乙酮、苯乙酸、2,6-二甲基吡嗪等12个关键差异香气成分,蒙特4号中引起香气特征变化的有雪松醇、2-甲基丁醛、4-乙烯基愈创木酚、愈创木酚、γ-壬内酯等11个关键差异香气成分。该研究结果反映了雪茄烟抽吸过程中烟气成分变化规律,并解释了抽吸过程中风味变化的原因。Abstract: In order to investigate the differences of aroma components and aroma profiles in segmented smoke of cigars, gas chromatography-mass spectrometry (GC-MS) was used to detect the aroma compounds of Great Wall No.2 and Montecristo No.4 cigars, supplemented by sensory evaluation and odor contribution weight to investigate the aroma characteristics of cigars, and the key aroma components in cigars were screened based on partial least squares discriminant analysis (PLS-DA). The results showed that the cigar was shorter, the interception effect was weakened, and the quantity and release of aroma components in cigar smoke were increased during smoking. In the odor contribution weight of segmented smoke of cigars, the bean and woody aromas of Great Wall No.2 weakened and the coffee aroma increased as smoking proceeded, while the bean aroma of Montecristo No.4 weakened and the spicy aroma increased. These changes in odor contribution weight were consistent with the results of the sensory evaluation. 12 key differential aroma components such as γ-hexalactone, 2-furoic acid, acetophenone, phenylacetic acid, 2,6-dimethylpyrazine were obtained during the smoking process of Great Wall No.2, and 11 key differential aroma components such as cedrol, 2-methylbutyraldehyde, 2-methoxy-4-vinylphenol, guaiacol, γ-nonanolactone were obtained during the smoking process of Montecristo No.4. The results of this study reflected the change rules of smoke composition in the smoking process of cigar and explained the reasons for the flavor changes in the smoking process of cigar.
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Key words:
- cigar /
- segmented smoke of cigar /
- aroma compound /
- aroma profile /
- odor contribution weight
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[1]
李爱军,秦艳青,代惠娟,等.国产雪茄烟叶科学发展刍议[J].中国烟草学报,2012,18(1):112-114.
-
[2]
闫新甫,王以慧,雷金山,等.国产雪茄分类探讨及其实际应用分析[J].中国烟草学报,2021,27(5):100-109.
-
[3]
帖金鑫,张青松,李永生,等.加拿大烟叶与云南KRK26烟叶香气成分差异分析[J].轻工学报,2023,38(5):74-82.
-
[4]
于航,刘砚婷,尚梦琦,等.基于致香成分分析的雪茄烟产地间差异[J].烟草科技,2021,54(9):58-71.
-
[5]
YAN T J,ZHOU P,LONG F,et al.Unraveling the difference in the composition/content of the aroma compounds in different tobacco leaves:For better use[J].Journal of Chemistry,2022,2022:3293899.
-
[6]
ZHENG T F,ZHANG Q Y,LI P H,et al.Analysis of microbial community,volatile flavor compounds,and flavor of cigar tobacco leaves from different regions[J].Frontiers in Microbiology,2022,13:907270.
-
[7]
施友志,潘勇,杜甫,等.基于SHS/GC-IMS、OAV值结合多元统计学的不同品种雪茄烟叶特征香气构成差异解析[J].分析测试学报,2023,42(6):674-683.
-
[8]
郭新枫.调制温湿度条件对雪茄外包皮烟叶生理变化与理化特性的影响[J].科技创新与应用,2013(21):4.
-
[9]
李一凡,赵松超,刘博远,等.采收时间对雪茄碳氮代谢关键酶活性和化学成分的影响[J].中国农业科技导报,2019,21(3):126-132.
-
[10]
姚芳,王慧方,徐世杰,等.施氮水平对海南茄衣中性致香物质含量的影响[J].中国农学通报,2017,33(16):83-90.
-
[11]
贾云,胡婉蓉,吕晋雄,等.雪茄烟叶发酵过程中微生物群落及功能微生物分析[J].轻工学报,2023,38(1):71-78
,89. -
[12]
胡婉蓉,蔡文,李东亮,等.发酵介质对雪茄烟叶化学成分及微生物群落结构的影响[J].轻工学报,2023,38(1):90-100.
-
[13]
李欣燕,王方玲,张明月,等.干旱胁迫下保水剂对雪茄烟叶碳氮代谢和中性香气物质含量的影响[J].浙江农业学报,2022,34(12):2610-2621.
-
[14]
张倩颖,罗诚,李东亮,等.雪茄烟叶调制及发酵技术研究进展[J].中国烟草学报,2020,26(4):1-6.
-
[15]
李秀妮,闫铁军,吴风光,等.全球主要产地雪茄烟叶的风味特征初探[J].中国烟草学报,2019,25(6):126-132.
-
[16]
胡军,余邦林,姬凌波,等.基于SHS-GC-MS和GC-IMS的对两种雪茄烟挥发性香味成分的分析与研究[J].中国烟草学报,2023,29(2):111-121.
-
[17]
朱贝贝,何声宝,安泓汋,等.国内外几种知名品牌雪茄化学及风格特征比较[J].中国烟草学报,2023,29(3):115-124.
-
[18]
余邦林,徐恒,姬凌波,等.国产雪茄烟挥发性成分质量分数和组成差异[J].烟草科技,2023,56(3):61-69.
-
[19]
国家烟草专卖局.雪茄烟 调节和测试的大气环境:YC/T 462—2013[S].北京:中国标准出版社,2013.
-
[20]
国家烟草专卖局.雪茄烟 用常规分析用雪茄烟吸烟机测定总粒相物和焦油:YC/T 463—2013[S].北京:中国标准出版社,2013.
-
[21]
吴金凤,张燕,高峄涵,等.不同烟支长度对加热卷烟烟气主要成分逐口释放量的影响[J].安徽农业科学,2023,51(7):200-203
,230. -
[22]
LEI H P,LIANG F Y,WANG Y G,et al.Simultaneous determination of thujopsene and cedrol in cedarwood oils from Platycladus orientalis and Thuja sutchuenensis by GC-MS[J].Journal of Essential Oil Bearing Plants,2011,14(1):48-56.
-
[23]
YANG P,SONG H L,WANG L J,et al.Characterization of key aroma-active compounds in black garlic by sensory-directed flavor analysis[J].Journal of Agricultural and Food Chemistry,2019,67(28):7926-7934.
-
[24]
FRANKLIN L M,KING E S,CHAPMAN D,et al.Flavor and acceptance of roasted california almonds during accelerated storage[J].Journal of Agricultural and Food Chemistry,2018,66(5):1222-1232.
-
[25]
XIAO L,LEE J,ZHANG G,et al.HS-SPME GC/MS characterization of volatiles in raw and dry-roasted almonds (Prunus dulcis)[J].Food Chemistry,2014,151:31-39.
-
[26]
VAN GEMERT L J.Compilations of odour threshold values in air, water and other media[M].2nd ed.Netherlands:Oliemans Punter & Partners BV,2011.
-
[27]
迟广俊,柴国璧,李小斌,等.卷烟主流烟气中吲哚和3-甲基吲哚的香气作用分析[J].烟草科技,2019,52(9):39-45.
-
[28]
CHEN C,LIU Z,YU H Y,et al.Characterization of six lactones in cheddar cheese and their sensory interactions studied by odor activity values and Feller's Additive Model[J].Journal of Agricultural and Food Chemistry,2022,70(1):301-308.
-
[29]
TAKOI K,DEGUEIL M,SHINKARUK S,et al.Investigation of the chemical compositions in tobacco of different origins and maturities at harvest by GC-MS and HPLC-PDA-QTOF-MS[J].Journal of Agricultural and Food Chemistry,2009,57(6):2493-2502.
-
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