JOURNAL OF LIGHT INDUSTRY

CN 41-1437/TS  ISSN 2096-1553

Volume 29 Issue 2
March 2014
Article Contents
FAN Ya-ling, WANG Da-feng, HE Yu-ping, et al. Determination of di(ethylene glycol) dibenzoate in water-based emulsion adhesives for cigarette with GC-MS method[J]. Journal of Light Industry, 2014, 29(2): 27-30. doi: 10.3969/j.issn.2095-476X.2014.02.008
Citation: FAN Ya-ling, WANG Da-feng, HE Yu-ping, et al. Determination of di(ethylene glycol) dibenzoate in water-based emulsion adhesives for cigarette with GC-MS method[J]. Journal of Light Industry, 2014, 29(2): 27-30. doi: 10.3969/j.issn.2095-476X.2014.02.008 shu

Determination of di(ethylene glycol) dibenzoate in water-based emulsion adhesives for cigarette with GC-MS method

  • Corresponding author: PENG Jun-cang, 
  • Received Date: 2014-01-02
    Available Online: 2014-03-15
  • In order to determine the content of di(ethylene glycol) dibenzoate(DEDB) in water-based emulsion adhesives for tobacco,the adhesives were extracted separately with n-hexane,cyclohexane,ethyl ether,2,2,4-trimethylpentane,and determined by GC-MS under selected ion monitoring mode.The results showed that oscillating time 40 min and extraction volume 10 mL were preferable duration for n-hexane extraction by adding 1 mL water into the sample;the calibration curves of the DEDB exhibited good linear relations(R2=0.999 4), the limits of detection 0.04 μg/mL,RSD=4.98%,and the recoveries ranged from 97%~101%.
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