JOURNAL OF LIGHT INDUSTRY

CN 41-1437/TS  ISSN 2096-1553

Volume 29 Issue 6
November 2014
Article Contents
ZHANG Ping-quan, XU Guang-zhong, DU Xiu-min, et al. Improvement of gas chromatography-mass spectrometry method for determination of phthalates in water-based adhesive[J]. Journal of Light Industry, 2014, 29(6): 9-12. doi: 10.3969/j.issn.2095-476X.2014.06.003
Citation: ZHANG Ping-quan, XU Guang-zhong, DU Xiu-min, et al. Improvement of gas chromatography-mass spectrometry method for determination of phthalates in water-based adhesive[J]. Journal of Light Industry, 2014, 29(6): 9-12. doi: 10.3969/j.issn.2095-476X.2014.06.003 shu

Improvement of gas chromatography-mass spectrometry method for determination of phthalates in water-based adhesive

  • Received Date: 2014-06-11
    Available Online: 2014-11-15
  • In order to raise efficiency and avoid equipment damage,the same capillary column of the benzene series in water-based adhesive was used to establish the method of determinating phthalates content in water-based adhesive.The results showed that the method had good reproducibility and accuracy,the variation coefficient was less than 6% and the average recovery ratio was 88.06%~104.26%.The range of detection limit and quantification limit were 0.002~0.027 μg/mL and 0.007~0.089 μg/mL respectively.There was not significant difference between the method and industry standard method,and the method could be used to determine the phthalates content in water-based adhesive.
  • 加载中
    1. [1]

      何凤生.中华职业医学[M].北京:人民卫生出版社,1999:434-533.

    2. [2]

      周国泰.危险化学品安全技术全书[M].北京:化学工业出版社,1997:17-18.

    3. [3]

      王民生.邻苯二甲酸酯(塑化剂)的毒性及对人体健康的危害[J].江苏预防医学,2011,22(4):68.

    4. [4]

      刘泽春,黄华发,刘江生,等.异丙醇萃取-气相色谱法同时测定烟用接装纸和包装纸中邻苯二甲酸酯类化合物[J].分析仪器,2010(2):30.

    5. [5]

      韩云辉,李旭华,叶长文,等.烟用拉线中邻苯二甲酸酯类物质的测定[J].郑州轻工业学院学报:自然科学版,2012,27(1):26.

    6. [6]

      郑向华,林立毅,方恩华,等.固相萃取-气相色谱-质谱法测定食品中23种邻苯二甲酸酯[J].色谱,2012,30(1):27.

    7. [7]

      李志伟,纪朋,马慧丽.塑料中邻苯二甲酸酯类化合物的GC/MS分析方法[J].郑州轻工业学院学报:自然科学版,2009,24(5):12.

    8. [8]

      黄惠贞,梁晖,刘秀彩.顶空-气质联用法分析水基胶中的苯系物[J].安徽农业科学,2012,27(40):13598.

Article Metrics

Article views(1386) PDF downloads(20) Cited by()

Ralated
    通讯作者: 陈斌, bchen63@163.com
    • 1. 

      沈阳化工大学材料科学与工程学院 沈阳 110142

    1. 本站搜索
    2. 百度学术搜索
    3. 万方数据库搜索
    4. CNKI搜索

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return