ZHANG Ping-quan, XU Guang-zhong, DU Xiu-min, et al. Improvement of gas chromatography-mass spectrometry method for determination of phthalates in water-based adhesive[J]. Journal of Light Industry, 2014, 29(6): 9-12. doi: 10.3969/j.issn.2095-476X.2014.06.003
Citation:
ZHANG Ping-quan, XU Guang-zhong, DU Xiu-min, et al. Improvement of gas chromatography-mass spectrometry method for determination of phthalates in water-based adhesive[J]. Journal of Light Industry, 2014, 29(6): 9-12.
doi:
10.3969/j.issn.2095-476X.2014.06.003
Improvement of gas chromatography-mass spectrometry method for determination of phthalates in water-based adhesive
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Huaiyin Cigarette Factory, China Tobacco Jiangsu Industrial Co., Ltd., Huaian 223002, China
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Received Date:
2014-06-11
Available Online:
2014-11-15
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Abstract
In order to raise efficiency and avoid equipment damage,the same capillary column of the benzene series in water-based adhesive was used to establish the method of determinating phthalates content in water-based adhesive.The results showed that the method had good reproducibility and accuracy,the variation coefficient was less than 6% and the average recovery ratio was 88.06%~104.26%.The range of detection limit and quantification limit were 0.002~0.027 μg/mL and 0.007~0.089 μg/mL respectively.There was not significant difference between the method and industry standard method,and the method could be used to determine the phthalates content in water-based adhesive.
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Proportional views
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