JOURNAL OF LIGHT INDUSTRY

CN 41-1437/TS  ISSN 2096-1553

Volume 32 Issue 1
January 2017
Article Contents
YU Jing-jing, PAN Li-ning, WANG Sheng, et al. Study on volatile carbonyl compounds in cigarette filter by HPLC-DAD technique and trapping efficiency[J]. Journal of Light Industry, 2017, 32(1): 35-42,64. doi: 10.3969/j.issn.2096-1553.2017.1.006
Citation: YU Jing-jing, PAN Li-ning, WANG Sheng, et al. Study on volatile carbonyl compounds in cigarette filter by HPLC-DAD technique and trapping efficiency[J]. Journal of Light Industry, 2017, 32(1): 35-42,64. doi: 10.3969/j.issn.2096-1553.2017.1.006 shu

Study on volatile carbonyl compounds in cigarette filter by HPLC-DAD technique and trapping efficiency

  • Received Date: 2016-03-05
    Available Online: 2017-01-15
  • A high performance liquid chromatography-diode array detector(HPLC-DAD)method was developed to determine volatile carbonyl compounds in cigarette filter including formaldehyde,acetaldehyde,propionaldehyde,acetone,acroein,crotonaldehyde,2-butanone and butyraldehyde.The cigarette filters were extracted by shaking with the mixed solution of acetonitrile and water(the volume ratio of 1: 1),then reacted with 2,4-dinitrophenylhydrazine,and analyzed by HPLC-DAD.The recoveries of 8 carbonyl compounds in cigarette filters were in the range of 80.8% and 115.7%.The precisions of intra-day and inter-day for formaldehyde,acetaldehyde and crotonaldehyde were good(RSD<10%).The trapping efficiency of carbonyl compounds in mainstream smoke for different kinds of cigarette filters was studied.The results showed that trapping efficiency of cigarette filter for total amounts of carbonyl compounds was low.Furthermore,formaldehyde and crotonaldehyde showed higher trapping efficiencies (>10%) compared with other carbonyl compounds(<7.0%).The trapping efficiencies of different types of cigarette filter to formaldehyde was activated carbon > acetate filter≈paper > polypropylene and that to crotonaldehyde was activated carbon > acetate filter > paper > polypropylene.
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    1. [1]

      李艳平,文建辉,彭斌,等.不同结构滤嘴的烟碱截留效率和空间分布模式[J].烟草科技,2013(2):57.

    2. [2]

      中国国家标准化管理委员会.卷烟滤嘴中烟碱的测定气相色谱法:YC/T 154-2001[S].北京:中国标准出版社,2001.

    3. [3]

      庹苏行,胡念念,戴云辉.LC-MS/MS法检测卷烟滤嘴截留的烟气TSNAs[J].烟草科技,2008(12):42.

    4. [4]

      于涛,张杰,曹建华,等.醋酸纤维滤嘴对卷烟主流烟气中主要酚类物质的选择性过滤研究[J].中国烟草学报,2009,15(3):25.

    5. [5]

      吴银菊,吴名剑,蒋腊梅,等.固相萃取-气相色谱/质谱同时测定卷烟滤嘴中的四种芳香胺[J].分析科学学报,2008,24(5):557.

    6. [6]

      王丽苹,任凤莲,吴名剑,等.固相萃取毛细管气相色谱法测定卷烟滤嘴中7种挥发性羰基化合物[J].分析试验室,2009,28(2):116.

    7. [7]

      王丽苹,任凤莲,吴名剑,等.不同材料滤嘴对卷烟主流烟气中挥发性羰基化合物截滤性能的研究[J].化学研究与应用,2008,20(6):796.

    8. [8]

      余晶晶,王昇,王冰,等.LC-ESI-MS-MS法检测卷烟滤嘴中8种挥发性羰基化合物[J].烟草科技,2013(9):36.

    9. [9]

      中国国家标准化管理委员会.卷烟主流烟气中主要羰基化合物的测定高效液相色谱法:YC/T 254-2008[S].北京:中国标准出版社,2008.

    10. [10]

      DONG J,MOLDOVEANU S C.Gas chromatography-mass spectrometry of carbonyl compounds in cigarette mainstream smoke after derivatization with 2,4-dinitrophenylhydrozine[J].J Chromatogr A,2004,1027(1/2):25.

    11. [11]

      谢复炜,吴鸣,王昇,等.卷烟主流烟气中羰基化合物的改进分析方法[J].中国烟草学报,2006,12(5):15.

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